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Effects of two wet exfoliation strategies on the yield and colloidal behavior of 2D hexagonal boron nitride nanosheets

Abstract We report the exfoliation process optimization, physicochemical characterizations, and comparative aggregation behavior of the inorganic 2D nanomaterial hexagonal Boron Nitride (h-BN) produced from two repetitive sonication-centrifugation processes with varying centrifugation speeds and recycle frequency: Continuous and Segmented protocols. Enhancing exfoliation efficiency and understanding aqueous stability are essential for sustainable design and environmental applications. Results showed that the Segmented protocol outperformed the Continuous protocol by having a six-fold increase in the exfoliated h-BN nanosheet yield by reusing the unexfoliated bulk h-BN and decreasing centrifugation speeds. Centrifugation speeds of 1880 and 950 rpm produced nanosheets of similar sizes due to the slight difference in the centrifugal force generated in both protocols. Moreover, nanosheets from both protocols had enhanced polarity due to …

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